N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

Base Information

Chemical Name:N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide
CAS No.:1323369-13-6
Molecular Formula:C₃₆H₃₈N₂O₂
Molecular Weight:530.71
Hs Code.:

Synonyms:N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

Suppliers and Price of N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

There total 2 articles about N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: N-(5-methyl-[1,1′-biphenyl]-2-yl)pivalamide

: 1323369-13-6
N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

Guidance literature:: With water; copper(II) bis(trifluoromethanesulfonate); bis(trifluoromethanesulfonyl)amide; Selectfluor; In 1,2-dichloro-ethane; at 120 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/anie.201101391

Reference yield:

: 87995-50-4
N-(2-bromo-4-methylphenyl)-2,2-dimethylpropanamide

: 98-80-6
phenylboronic acid

: 1323369-13-6
N-(5-(2-tert-butyl-6-methyl-8-phenyl-4H-benzo[d][1,3]oxazin-4-yl)biphenyl-2-yl)pivalamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.33 h / 20 °C / Inert atmosphere

1.2: 80 °C / Inert atmosphere

2.1: water; copper(II) bis(trifluoromethanesulfonate); bis(trifluoromethanesulfonyl)amide; Selectfluor / 1,2-dichloro-ethane / 1.5 h / 120 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; copper(II) bis(trifluoromethanesulfonate); bis(trifluoromethanesulfonyl)amide; Selectfluor; In 1,2-dimethoxyethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201101391