cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

Base Information

Chemical Name:cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane
CAS No.:173437-87-1
Molecular Formula:C₂₁H₃₉N₃O₆
Molecular Weight:429.557
Hs Code.:

Synonyms:cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

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Chemical Property of cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

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Technology Process of cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

There total 3 articles about cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 105-36-2
ethyl bromoacetate

: 173437-79-1
cis-cis-2,4,6-trimethyl-1,3,5-triaminocyclohexane

: 173437-87-1
cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1039/C39950002361

Reference yield:

: 602-96-0
2,4,6-trinitromesitylene

: 173437-87-1
cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaBH₄, Cu(OAc)2 / aq. ethanol

2: H₂ / Rh/Pd / aq. H₂SO₄ / 144 h / 20 °C / 2280 Torr

3: 83 percent / Cs₂CO₃ / dimethylformamide / 60 °C

With sodium tetrahydroborate; copper diacetate; hydrogen; caesium carbonate; Rh/Pd; In ethanol; sulfuric acid; N,N-dimethyl-formamide;
DOI:10.1039/C39950002361

Reference yield:

: 4380-92-1
1,3,5-trisamine-2,4,6-trimethylbenzene

: 173437-87-1
cis,cis-1,3,5-tris(ethoxycarbonylmethylamino)-2,4,6-trimethylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Rh/Pd / aq. H₂SO₄ / 144 h / 20 °C / 2280 Torr

2: 83 percent / Cs₂CO₃ / dimethylformamide / 60 °C

With hydrogen; caesium carbonate; Rh/Pd; In sulfuric acid; N,N-dimethyl-formamide;
DOI:10.1039/C39950002361