2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

Base Information

Chemical Name:2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide
CAS No.:1448536-67-1
Molecular Formula:C₁₇H₂₈N₂O₃S₂
Molecular Weight:372.553
Hs Code.:

Synonyms:2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

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Chemical Property of 2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

Chemical Property:

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Technology Process of 2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

There total 4 articles about 2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: (E)-2-methyl-N-(4-(piperidin-1-ylsulfonyl)benzylidene)propane-2-sulfinamide

: 917-54-4
methyllithium

: 1448536-67-1
2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - 25 ℃; for 17h;
DOI:10.1021/jm4008664

Reference yield:

: 85822-16-8
4-formylbenzene-1-sulfonyl chloride

: 1448536-67-1
2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C

2: titanium(IV) tetraethanolate / tetrahydrofuran / 2 h / 25 °C / Inert atmosphere

3: tetrahydrofuran; diethyl ether / 17 h / -78 - 25 °C

With titanium(IV) tetraethanolate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm4008664

Reference yield:

: 110-89-4
piperidine

: 1448536-67-1
2-methyl-N-(1-(4-(piperidin-1-ylsulfonyl)phenyl)ethyl)propane-2-sulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C

2: titanium(IV) tetraethanolate / tetrahydrofuran / 2 h / 25 °C / Inert atmosphere

3: tetrahydrofuran; diethyl ether / 17 h / -78 - 25 °C

With titanium(IV) tetraethanolate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm4008664