1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid

Base Information

Chemical Name:1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid
CAS No.:71176-75-5
Molecular Formula:C₁₁H₁₆INO₄S
Molecular Weight:385.223
Hs Code.:

Synonyms:1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid

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Technology Process of 1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid

There total 4 articles about 1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.9%

: 71176-74-4
1-<5-(1,1-dimethylethyl)-2-hydroxyphenyl>methanesulfamic acid

: 71176-75-5
1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid

Guidance literature:: With Iodine monochloride; In hydrogenchloride; water-tetrahydrofuran;

Reference yield:

: 2725-53-3
2-hydroxy-5-t-butylbenzaldehyde

: 71176-75-5
1-<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methanesulfamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ammonium sulfamate, 2.) NaBH₄ / 1.) MeOH, reflux, 1.5 h, 2.) MeOH, 20 deg C, 20 h

2: ICl / H₂O; tetrahydrofuran

With sodium tetrahydroborate; ammonium sulfamate; Iodine monochloride; In tetrahydrofuran; water;
DOI:10.1021/jm00348a024