[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

Base Information

Chemical Name:[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine
CAS No.:1280733-79-0
Molecular Formula:C₁₈H₁₃BrN₄O₂
Molecular Weight:397.231
Hs Code.:

Synonyms:[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

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Chemical Property of [5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

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Technology Process of [5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

There total 3 articles about [5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 613-94-5
benzoic acid hydrazide

: 91182-60-4
5-(4-bromophenyl)-3-methylisoxazole-4-carboxylic acid

: 1280733-79-0
[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

Guidance literature:: 5-(4-bromophenyl)-3-methylisoxazole-4-carboxylic acid; With diphenylphosphoranyl azide; triethylamine; In toluene; at 60 ℃; for 0.333333h;

benzoic acid hydrazide; In toluene; for 2h; Heating;

With trichlorophosphate; In 1,4-dioxane; at 100 ℃;

Reference yield:

: 85963-90-2
methyl 2-(4-bromobenzoyl)-3-oxo-butanoate

: 1280733-79-0
[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; acetic acid / 1 h / 115 °C

2.1: water; lithium hydroxide / methanol / 1 h / 60 °C

3.1: triethylamine; diphenylphosphoranyl azide / toluene / 0.33 h / 60 °C

3.2: 2 h / Heating

3.3: 100 °C

With diphenylphosphoranyl azide; hydroxylamine hydrochloride; water; acetic acid; triethylamine; lithium hydroxide; In methanol; toluene;

Reference yield:

: 1228689-61-9
methyl 5-(4-bromophenyl)-3-methylisoxazole-4-carboxylate

: 1280733-79-0
[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-(5-phenyl-[1,3,4]oxadiazol-2-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; lithium hydroxide / methanol / 1 h / 60 °C

2.1: triethylamine; diphenylphosphoranyl azide / toluene / 0.33 h / 60 °C

2.2: 2 h / Heating

2.3: 100 °C

With diphenylphosphoranyl azide; water; triethylamine; lithium hydroxide; In methanol; toluene;