N-cyclohexyl-N-hexylbenzamide

Base Information

Chemical Name:N-cyclohexyl-N-hexylbenzamide
CAS No.:94438-89-8
Molecular Formula:C₁₉H₂₉NO
Molecular Weight:287.445
Hs Code.:

Synonyms:N-cyclohexyl-N-hexylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-N-hexylbenzamide

Chemical Property:

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Technology Process of N-cyclohexyl-N-hexylbenzamide

There total 2 articles about N-cyclohexyl-N-hexylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cyclohexyl-hexyl-amine; hydrochloride

: 98-88-4
benzoyl chloride

: 94438-89-8
N-cyclohexyl-N-hexylbenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jacs.1c03644

Reference yield:

: 592-41-6,25067-06-5
1-hexene

: 108-91-8,157973-60-9
cyclohexylamine

: 94438-89-8
N-cyclohexyl-N-hexylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,4,6-Triisopropylthiophenol; 1,2-bis(2,4,6-triisopropylphenyl)disulfane; [Ir(3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl)₂(4,4'-bis(trifluoromethyl)bipyridine)]PF₆ / dichloromethane / 20 °C / Irradiation; Flow reactor; Inert atmosphere

1.2: 0.17 h / Inert atmosphere

2.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With 1,2-bis(2,4,6-triisopropylphenyl)disulfane; 2,4,6-Triisopropylthiophenol; [Ir(3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl)₂(4,4'-bis(trifluoromethyl)bipyridine)]PF₆; triethylamine; In dichloromethane;
DOI:10.1021/jacs.1c03644