4-benzoyltetrachloropyridine

Base Information

• Chemical Name: 4-benzoyltetrachloropyridine
• CAS No.: 18613-89-3
• Molecular Formula: C₁₂H₅Cl₄NO
• Molecular Weight: 320.99
• Mol file: 18613-89-3.mol

Synonyms:4-benzoyltetrachloropyridine

Chemical Property of 4-benzoyltetrachloropyridine

Chemical Property:

Purity/Quality:

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Technology Process of 4-benzoyltetrachloropyridine

There total 5 articles about 4-benzoyltetrachloropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

tetrachloro-4-pyridylcopper (27425-94-1) + benzoyl chloride (98-88-4) → 2,3,5,6-tetrachloropyridine (2402-79-1) + 4-benzoyltetrachloropyridine (18613-89-3)

Guidance literature:

In N,N-dimethyl-formamide; for 0.5h; Heating;

DOI:10.1039/P19800001682

Reference yield: 2.5%

tetrachloro-4-pyridylcopper (27425-94-1) + benzoyl chloride (98-88-4) → 2,3,5,6-tetrachloropyridine (2402-79-1) + 4-benzoyltetrachloropyridine (18613-89-3) + 2,3,4,5,6-pentachloropyridine (2176-62-7) + octachloro-4,4'-bipyridyl (18725-60-5)

Guidance literature:

With para-xylene; In N,N-dimethyl-formamide; for 23h; Product distribution; Mechanism; Heating; the similar reaction without p-xylene; other reaction times; similar range of products to those obtained from 4-bromotetrachloropyridine;

DOI:10.1039/P19800001682

Reference yield: 1.0%

tetrachloro-4-pyridylcopper (27425-94-1) → 2,3,5,6-tetrachloropyridine (2402-79-1) + 4-benzoyltetrachloropyridine (18613-89-3) + 2,3,4,5,6-pentachloropyridine (2176-62-7) + octachloro-4,4'-bipyridyl (18725-60-5)

Guidance literature:

With para-xylene; benzoyl chloride; In N,N-dimethyl-formamide; for 23h; Heating;

DOI:10.1039/P19800001682

upstream raw materials:

tetrachloro-4-pyridylcopper

benzoyl chloride

tetrachloro-4-pyridylmagnesium chloride