6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol)

Base Information

• Chemical Name: 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol)
• CAS No.: 812693-91-7
• Molecular Formula: C₃₆H₅₈N₂O₂
• Molecular Weight: 550.869

Synonyms:6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol)

Chemical Property of 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol)

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Technology Process of 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol)

There total 6 articles about 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine (151433-25-9) → 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol) (812693-91-7)

Guidance literature:

With sodium tetrahydroborate; acetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.201701289

Reference yield: 90.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,4-di-tert-Butylphenol (96-76-4) + (1R,2R)-1,2-diaminocyclohexane tartrate (32044-22-7,39961-95-0) → 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol) (812693-91-7)

Guidance literature:

With potassium carbonate; In ethanol; water; for 2.5h; Heating;

DOI:10.1016/S0040-4039(01)01264-3

Reference yield:

(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine (135616-40-9) → 6,6′-({[(1R,2R)-cyclohexane-1,2-diyl]bis(azanediyl)}bis-[methylene])bis(2,4-di-tert-butylphenol) (812693-91-7)

Guidance literature:

With sodium tetrahydroborate; In methanol; Heating;

DOI:10.1021/jo040221d

upstream raw materials:

formaldehyd

2,4-di-tert-Butylphenol

(1R,2R)-1,2-diaminocyclohexane tartrate

(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine

Downstream raw materials:

(1R,2R)-N,N′-dimethyl-N,N′-di[(2-hydroxy-3,5-di(tert-butyl))benzyl]-1,2-diaminocyclohexane

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