N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester

Base Information

• Chemical Name: N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester
• CAS No.: 232614-92-5
• Molecular Formula: C₁₇H₂₅N₃O₄
• Molecular Weight: 335.403

Synonyms:N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester

Chemical Property of N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester

There total 3 articles about N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butoxycarbonyl-N-methyl-D-phenylalanine (37553-65-4,64263-83-8,85466-66-6) + acetic acid hydrazide (1068-57-1) → N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester (232614-92-5)

Guidance literature:

N-tert-butoxycarbonyl-N-methyl-D-phenylalanine; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; for 0.333333h;

acetic acid hydrazide; With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0223-5234(00)00146-X

Reference yield:

→ N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester (232614-92-5)

Guidance literature:

Reference yield:

→ N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester + N-[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamic acid tert-butyl ester (232614-92-5)

Guidance literature:

upstream raw materials:

N-tert-butoxycarbonyl-N-methyl-D-phenylalanine

acetic acid hydrazide

Downstream raw materials:

{4-[(1-{[2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethyl]-methyl-carbamoyl}-2-naphthalen-2-yl-ethyl)-methyl-carbamoyl]-1,1-dimethyl-but-3-enyl}-carbamic acid tert-butyl ester

N-((1R)-1-(N[(1R)-2-(N'-acetylhydrazino)-1-benzyl-2-oxoethyl]-N-methylcarbamoyl)-2-(2-naphthyl)ethyl)-N-methylcarbamic acid tert-butyl ester

N-[2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethyl]-N-methyl-2-methylamino-3-naphthalen-2-yl-propionamide

acetic acid N'-((2R)-2-(methylamino)-3-phenylpropionyl)hydrazide

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