1',3'-dohexadecyl N--L-glutamate

Base Information

Chemical Name:1',3'-dohexadecyl N--L-glutamate
CAS No.:171195-66-7
Molecular Formula:C₄₇H₈₀N₂O₉
Molecular Weight:817.16
Hs Code.:

1',3'-dohexadecyl N-<O-(4-nitrophenyl)succinyl>-L-glutamate

Synonyms:1',3'-dohexadecyl N--L-glutamate

Suppliers and Price of 1',3'-dohexadecyl N--L-glutamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1',3'-dohexadecyl N--L-glutamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1',3'-dohexadecyl N--L-glutamate

There total 5 articles about 1',3'-dohexadecyl N--L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 125401-63-0
N-succinyl-Glu^inv(OC₁₆H₃₃)-OC₁₆H₃₃

: 171195-66-7
1',3'-dohexadecyl N--L-glutamate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; 1.) 2 h, 2.) RT, 24 h;
DOI:10.1021/ja00142a019

Reference yield:

: 59274-90-7
1',3'-dihexadecyl L-glutamate

: 171195-66-7
1',3'-dohexadecyl N--L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine / tetrahydrofuran; CHCl₃ / 4 h / 30 °C

2: 85 percent / N,N-dicyclohexylcarbodiimide, (dimethylamino)pyridine / CH₂Cl₂ / 1.) 2 h, 2.) RT, 24 h

With dmap; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1021/ja00142a019

Reference yield:

: 56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
L-glutamic acid

: 171195-66-7
1',3'-dohexadecyl N--L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / toluene / Heating

2: 94 percent / triethylamine / tetrahydrofuran; CHCl₃ / 4 h / 30 °C

3: 85 percent / N,N-dicyclohexylcarbodiimide; (dimethylamino)pyridine / CH₂Cl₂ / 26 h / 0 - 20 °C

With dmap; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; chloroform; toluene; 1: Esterification / 2: Acylation / 3: Esterification;
DOI:10.1016/S0968-0896(98)00216-8