benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Base Information

Chemical Name:benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate
CAS No.:49626-54-2
Molecular Formula:C₁₅H₁₈N₂O₃S
Molecular Weight:306.386
Hs Code.:

Synonyms:benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

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Chemical Property of benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

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Technology Process of benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

There total 22 articles about benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1316164-07-4
benzyl (2S,5R,6S)-3,3-dimethyl-7-oxo-6-phthalisoimido-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

: 49626-54-2
benzyl (2S,5R,6S)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; toluene; at 20 ℃; for 24h; Irradiation; Inert atmosphere;
DOI:10.1039/c7nj03557h

Reference yield: 65.0%

: 551-16-6
6-Aminopenicillanic Acid

: 100-39-0
benzyl bromide

: 3956-31-8,49626-54-2,64519-71-7
benzyl (2S,5R,6R)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: With dmap; triethylamine; In acetone; at 20 ℃; for 48h;
DOI:10.1515/znb-2007-1116

Reference yield:

: C₂₀H₂₄N₂O₅S

: 3956-31-8,49626-54-2,64519-71-7
benzyl (2S,5R,6R)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: C₂₀H₂₄N₂O₅S; With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 0.166667h;

With triethylamine; In dichloromethane; for 2h; Inert atmosphere;
DOI:10.3390/molecules201219828