5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

Base Information

Chemical Name:5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde
CAS No.:178749-81-0
Molecular Formula:C₃₇H₃₂O₆
Molecular Weight:572.657
Hs Code.:

Synonyms:5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

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Chemical Property of 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

Chemical Property:

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Technology Process of 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

There total 10 articles about 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 247086-81-3
(4-benzyloxy-2-hydroxymethyl-6-methoxy-phenyl)-(2,6-bis-benzyloxy-4-methyl-phenyl)-methanone

: 178749-81-0
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(99)00305-4

Reference yield:

: 100-39-0
benzyl bromide

: 178749-81-0
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 33 percent / K₂CO₃ / acetonitrile / Heating

2: 96 percent / K₂CO₃ / acetonitrile / Heating

3: 96 percent / LiAlH₄ / tetrahydrofuran

4: 43 percent / NBS / CCl₄

5: 82 percent / DEAD, PPh₃ / tetrahydrofuran

6: 45 percent / n-BuLi / tetrahydrofuran / -78 °C

7: 54 percent / PDC / dimethylformamide

With N-Bromosuccinimide; lithium aluminium tetrahydride; dipyridinium dichromate; n-butyllithium; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(99)00305-4

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 178749-81-0
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 33 percent / K₂CO₃ / acetonitrile / Heating

2: 96 percent / K₂CO₃ / acetonitrile / Heating

3: 96 percent / LiAlH₄ / tetrahydrofuran

4: 43 percent / NBS / CCl₄

5: 82 percent / DEAD, PPh₃ / tetrahydrofuran

6: 45 percent / n-BuLi / tetrahydrofuran / -78 °C

7: 54 percent / PDC / dimethylformamide

With N-Bromosuccinimide; lithium aluminium tetrahydride; dipyridinium dichromate; n-butyllithium; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(99)00305-4