5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Base Information

Chemical Name:5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid
CAS No.:247086-79-9
Molecular Formula:C₃₇H₃₂O₇
Molecular Weight:588.657
Hs Code.:

Synonyms:5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Suppliers and Price of 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

There total 11 articles about 5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 178749-81-0
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzaldehyde

: 247086-79-9
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Guidance literature:: With pyridine; potassium permanganate; Bu₄(NH₄); In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(99)00305-4

Reference yield:

: 100-39-0
benzyl bromide

: 247086-79-9
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: 33 percent / K₂CO₃ / acetonitrile / Heating

2: 96 percent / K₂CO₃ / acetonitrile / Heating

3: 96 percent / LiAlH₄ / tetrahydrofuran

4: 43 percent / NBS / CCl₄

5: 82 percent / DEAD, PPh₃ / tetrahydrofuran

6: 45 percent / n-BuLi / tetrahydrofuran / -78 °C

7: 54 percent / PDC / dimethylformamide

8: 81 percent / Bu₄(NH₄), KMnO₄, pyridine / dimethylformamide

With pyridine; potassium permanganate; N-Bromosuccinimide; lithium aluminium tetrahydride; dipyridinium dichromate; n-butyllithium; Bu₄(NH₄); potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(99)00305-4

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 247086-79-9
5-benzyloxy-2-(2,6-bis-benzyloxy-4-methyl-benzoyl)-3-methoxy-benzoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: 33 percent / K₂CO₃ / acetonitrile / Heating

2: 96 percent / K₂CO₃ / acetonitrile / Heating

3: 96 percent / LiAlH₄ / tetrahydrofuran

4: 43 percent / NBS / CCl₄

5: 82 percent / DEAD, PPh₃ / tetrahydrofuran

6: 45 percent / n-BuLi / tetrahydrofuran / -78 °C

7: 54 percent / PDC / dimethylformamide

8: 81 percent / Bu₄(NH₄), KMnO₄, pyridine / dimethylformamide

With pyridine; potassium permanganate; N-Bromosuccinimide; lithium aluminium tetrahydride; dipyridinium dichromate; n-butyllithium; Bu₄(NH₄); potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(99)00305-4