benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

Base Information

Chemical Name:benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate
CAS No.:1043504-43-3
Molecular Formula:C₂₉H₃₄NO₇P
Molecular Weight:539.565
Hs Code.:

Synonyms:benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

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Chemical Property of benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

Chemical Property:

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Technology Process of benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

There total 8 articles about benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 30379-58-9
benzyl glycolate

: 106019-45-8
benzyl hydrogen [(R,S)-1-(benzyloxycarbonylamino)pent-1-yl]phosphonate

: 1043504-43-3
benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

Guidance literature:: With TEA; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tetlet.2008.05.028

Reference yield:

: 80088-88-6
[(R,S)-1-(benzyloxycarbonylamino)pentyl]phosphonic acid

: 1043504-43-3
benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; benzene / 12 h / 80 °C

2: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 12 h / 80 °C

3: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1016/j.tet.2009.05.051

Reference yield:

: 1043504-42-2
dibenzyl [(R,S)-1-(benzyloxycarbonylamino)pentyl]phosphonate

: 1043504-43-3
benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(benzyloxy)phosphoryl]oxy}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 12 h / 80 °C

2: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2009.05.051