methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

Base Information

Chemical Name:methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate
CAS No.:131925-06-9
Molecular Formula:C₂₃H₂₃N₃O₄
Molecular Weight:405.453
Hs Code.:

Synonyms:methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

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Chemical Property of methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

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Technology Process of methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

There total 5 articles about methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 131925-03-6
Methyl 5-methyl-10,11-dihydro-5H-pyrrolo<1,2-b><1,2,5>benzotriazepine-11-acetate

: 100-07-2
4-methoxy-benzoyl chloride

: 131925-06-9
methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 72h; Heating;

Reference yield:

: 87948-04-7
N-methyl-N-(2-aminophenyl)-1H-pyrrol-1-ylamine

: 131925-06-9
methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / tetrahydrofuran / 15 h / Ambient temperature

2: 74 percent / POCl₃ / CH₂Cl₂ / 20 h / Heating

3: 90 percent / NaBH₃CN, HCl / ethanol; tetrahydrofuran / 20 h / Ambient temperature

4: 80 percent / Et₃N / tetrahydrofuran / 72 h / Heating

With hydrogenchloride; sodium cyanoborohydride; triethylamine; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 131925-12-7
5-Methyl-11-methoxycarbonylmethylene-5H,10H-pyrrolo<1,2-b><1,2,5>benzotriazepine

: 131925-06-9
methyl 10,11-dihydro-5-methyl-10-(4-methoxybenzoyl)-5H-pyrrolo[1,2-b][1,2,5]-benzotriazepine-11-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaBH₃CN, HCl / ethanol; tetrahydrofuran / 20 h / Ambient temperature

2: 80 percent / Et₃N / tetrahydrofuran / 72 h / Heating

With hydrogenchloride; sodium cyanoborohydride; triethylamine; In tetrahydrofuran; ethanol;