N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

Base Information

Chemical Name:N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)
CAS No.:1426686-02-3
Molecular Formula:C₃₄H₄₆N₄O₁₀S₂
Molecular Weight:734.892
Hs Code.:

Synonyms:N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

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Chemical Property of N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

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Technology Process of N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

There total 4 articles about N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.05%

: 936074-44-1
5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzene-1-sulfonyl chloride

: 68960-97-4,892154-56-2
1,14-diamino-3,6,9,12-tetraoxatetradecane

: 1426686-02-3
N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

Guidance literature:: With pyridine; at 20 ℃; for 12h;

Reference yield:

: 10557-85-4
4-iodo-3,5-dimethylisoxazole

: 1426686-02-3
N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 12 h / 85 °C / Inert atmosphere

2: chlorosulfonic acid; phosphorus pentachloride / dichloromethane / 0 - 70 °C / Inert atmosphere

3: pyridine / 6 h / 20 °C

With chlorosulfonic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus pentachloride; sodium carbonate; In 1,4-dioxane; pyridine; dichloromethane;

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 1426686-02-3
N,N'-(3,6,9,12-tetraoxatetradecane-1,14-diyl)bis(5-(3,5-dimethylisoxazol-4-yl)-2-methylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 12 h / 85 °C / Inert atmosphere

2: chlorosulfonic acid; phosphorus pentachloride / dichloromethane / 0 - 70 °C / Inert atmosphere

3: pyridine / 6 h / 20 °C

With chlorosulfonic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus pentachloride; sodium carbonate; In 1,4-dioxane; pyridine; dichloromethane;