4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid

Base Information

Chemical Name:4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid
CAS No.:676517-65-0
Molecular Formula:C₂₅H₃₀Cl₂N₂O₃
Molecular Weight:477.431
Hs Code.:

Synonyms:4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid

Chemical Property:

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Technology Process of 4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid

There total 2 articles about 4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 676517-39-8
4-(3,4-dichlorophenoxy)-1-(piperidin-4-ylmethyl)piperidine

: 298-12-4
Glyoxilic acid

: 98-80-6
phenylboronic acid

: 676517-65-0
4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid

Guidance literature:: In ethanol; water; at 100 ℃; for 0.0833333h;

Reference yield:

: 245057-73-2
4-(3,4-dichloro-phenoxy)-piperidine

: 50675-20-2
piperidine-4-carbaldehyde

: 298-12-4
Glyoxilic acid

: 98-80-6
phenylboronic acid

: 676517-65-0
4-[[4-(3,4-dichlorophenoxy)-1-piperidinyl]methyl]-α-phenyl-1-piperidineacetic acid

Guidance literature:: 4-(3,4-dichloro-phenoxy)-piperidine; piperidine-4-carbaldehyde; With sodium triacetoxy borohydride; acetic acid; In dichloromethane; at 20 ℃; for 18h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 16h;

Glyoxilic acid; phenylboronic acid; In ethanol; dichloromethane; at 100 ℃; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.08.103