C₂₃H₂₈N₄O₅

Base Information

Chemical Name:C₂₃H₂₈N₄O₅
CAS No.:210699-84-6
Molecular Formula:C₂₃H₂₈N₄O₅
Molecular Weight:440.499
Hs Code.:

C<sub>23</sub>H<sub>28</sub>N<sub>4</sub>O<sub>5</sub>

Synonyms:C₂₃H₂₈N₄O₅

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Chemical Property of C₂₃H₂₈N₄O₅

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Technology Process of C₂₃H₂₈N₄O₅

There total 10 articles about C₂₃H₂₈N₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111005-65-3
(-)-2,3-(cyclohexylidenedioxy)-4-cyclopentenone

: 210699-84-6
C₂₃H₂₈N₄O₅

Guidance literature:: Multi-step reaction with 10 steps

1: 50 percent / benzophenone / 2 h / Irradiation

2: 1.28 g / pyridine / 3 h / Ambient temperature

3: 78 percent / NaBH₄, CeCl₃*7H₂O / methanol / 0.08 h / 0 °C

4: 100 percent / pyridine / 2 h / 0 - 20 °C

5: 81 percent / sodium azide / dimethylformamide / 20 h / 120 °C

6: 81 percent / H₂ / 10percent Pd/C / methanol / 20 h / 760 Torr / Ambient temperature

7: 0.30 g / benzene / 0.5 h / 10 °C

8: 60 percent / conc. aq. NH₄OH / dimethylformamide / 4 h / 110 °C

9: Et₃N, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

10: hydrazine / dioxane / 1 h / Ambient temperature

With pyridine; dmap; ammonium hydroxide; sodium tetrahydroborate; sodium azide; benzophenone; cerium(III) chloride; hydrogen; triethylamine; hydrazine; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm980111x

Reference yield:

: 98-88-4
benzoyl chloride

: 210699-84-6
C₂₃H₂₈N₄O₅

Guidance literature:: Multi-step reaction with 9 steps

1: 1.28 g / pyridine / 3 h / Ambient temperature

2: 78 percent / NaBH₄, CeCl₃*7H₂O / methanol / 0.08 h / 0 °C

3: 100 percent / pyridine / 2 h / 0 - 20 °C

4: 81 percent / sodium azide / dimethylformamide / 20 h / 120 °C

5: 81 percent / H₂ / 10percent Pd/C / methanol / 20 h / 760 Torr / Ambient temperature

6: 0.30 g / benzene / 0.5 h / 10 °C

7: 60 percent / conc. aq. NH₄OH / dimethylformamide / 4 h / 110 °C

8: Et₃N, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

9: hydrazine / dioxane / 1 h / Ambient temperature

With pyridine; dmap; ammonium hydroxide; sodium tetrahydroborate; sodium azide; cerium(III) chloride; hydrogen; triethylamine; hydrazine; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm980111x

Reference yield:

: 175845-88-2
(2R,3R,4R)-4-hydroxymethyl-2,3-(cyclohexylidenedioxy)-1-cyclopentanone

: 210699-84-6
C₂₃H₂₈N₄O₅

Guidance literature:: Multi-step reaction with 9 steps

1: 1.28 g / pyridine / 3 h / Ambient temperature

2: 78 percent / NaBH₄, CeCl₃*7H₂O / methanol / 0.08 h / 0 °C

3: 100 percent / pyridine / 2 h / 0 - 20 °C

4: 81 percent / sodium azide / dimethylformamide / 20 h / 120 °C

5: 81 percent / H₂ / 10percent Pd/C / methanol / 20 h / 760 Torr / Ambient temperature

6: 0.30 g / benzene / 0.5 h / 10 °C

7: 60 percent / conc. aq. NH₄OH / dimethylformamide / 4 h / 110 °C

8: Et₃N, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

9: hydrazine / dioxane / 1 h / Ambient temperature

With pyridine; dmap; ammonium hydroxide; sodium tetrahydroborate; sodium azide; cerium(III) chloride; hydrogen; triethylamine; hydrazine; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm980111x