N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

Base Information

Chemical Name:N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester
CAS No.:148715-93-9
Molecular Formula:C₃₁H₃₇N₄O₆PS
Molecular Weight:624.698
Hs Code.:

Synonyms:N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

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Chemical Property of N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

Chemical Property:

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Technology Process of N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

There total 8 articles about N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62056-86-4
N-(diphenylphosphinoyl)glycine

: 148715-93-9
N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / CH₂Cl₂ / 0.25 h / -5 °C

2: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 2491-18-1
(S)-methyl 2-amino-4-(methylthio)butanoate hydrochloride

: 148715-93-9
N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: N-methylmorpholine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) to r. t., 1 h

2: HCl / methanol / 2 h

3: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

4: 86 percent / HCl / methanol / 0.5 h / 35 °C

5: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 22248-60-8
L-phenylalanyl-L-methionine methyl ester

: 148715-93-9
N-(diphenylphosphinoyl)glycylglycylphenylalanylmethionine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

2: 86 percent / HCl / methanol / 0.5 h / 35 °C

3: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; In methanol; dichloromethane; N,N-dimethyl-formamide;