C₃₃H₄₂O₉Si

Base Information

Chemical Name:C₃₃H₄₂O₉Si
CAS No.:1313275-59-0
Molecular Formula:C₃₃H₄₂O₉Si
Molecular Weight:610.777
Hs Code.:

C<sub>33</sub>H<sub>42</sub>O<sub>9</sub>Si

Synonyms:C₃₃H₄₂O₉Si

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Chemical Property of C₃₃H₄₂O₉Si

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Technology Process of C₃₃H₄₂O₉Si

There total 29 articles about C₃₃H₄₂O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1313275-24-9
C₃₅H₄₆O₈Si

: 1313275-59-0
C₃₃H₄₂O₉Si

Guidance literature:: With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; In tetrahydrofuran; water; at 0 - 23 ℃; for 2h;

Reference yield: 69.0%

: C₃₅H₄₆O₈Si

: 1313275-59-0
C₃₃H₄₂O₉Si

Guidance literature:: With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; at 0 ℃;
DOI:10.1073/pnas.1015257108

Reference yield:

: 1313275-47-6
(2S)-2-(tert-butyldimethylsilyloxy)-4-hydroxy-N-methoxy-N-methylbutanamide

: 1313275-59-0
C₃₃H₄₂O₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate; sodium hypochlorite / potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 0.25 h / 23 °C

2.1: C₁₃H₁₈NO₂^(1-)*Li⁽¹⁺⁾ / toluene; hexane / 1.33 h / 0 °C / Inert atmosphere

2.2: 6 h / -70 - 10 °C

3.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 0.5 h / 23 °C

4.1: tetrahydrofuran / 2 h / 0 °C

5.1: Hoveyda-Grubbs catalyst second generation / benzene / 0.67 h / 23 °C / Inert atmosphere; Heating

6.1: lithium tert-butoxide / tetrahydrofuran / 0.08 h / -78 °C

6.2: 2.5 h / -78 - -22 °C

6.3: 4.5 h / -22 - 23 °C

7.1: 2,6-dimethylpyridine; sodium periodate; potassium osmate(VI) dihydrate / water; tetrahydrofuran / 2 h / 0 - 23 °C

With 2,6-dimethylpyridine; C₁₃H₁₈NO₂^(1-)*Li⁽¹⁺⁾; potassium osmate(VI) dihydrate; sodium hypochlorite; sodium periodate; sodium hydrogencarbonate; lithium tert-butoxide; Hoveyda-Grubbs catalyst second generation; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; hexane; dichloromethane; water; toluene; benzene;