2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Base Information

Chemical Name:2-(2-Hydroxyphenyl)-2-methoxyessigsaeure
CAS No.:75335-12-5
Molecular Formula:C₉H₁₀O₄
Molecular Weight:182.176
Hs Code.:

Synonyms:2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Suppliers and Price of 2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

There total 6 articles about 2-(2-Hydroxyphenyl)-2-methoxyessigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: diethyl 2-(2-hydroxyphenyl)-2-methoxymalonate

: 75335-12-5
2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Guidance literature:: With lithium hydroxide; In methanol; water; at 20 ℃; for 5h;
DOI:10.1039/c5cc00354g

Reference yield:

: 67-56-1
methanol

: 75335-00-1
2-Methoxy-2-(4-methoxybenzoyl)-3(2H)-benzofuranon

: 121-98-2
methyl 4-methoxybenzoate

: 63697-51-8
2-(o-Hydroxyphenyl)-2-methoxyessigsaeuremethylester

: 75335-12-5
2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Guidance literature:: With hydrogenchloride; at 80 ℃; for 50h; Yield given. Yields of byproduct given;

Reference yield:

: 98-80-6
phenylboronic acid

: 75335-12-5
2-(2-Hydroxyphenyl)-2-methoxyessigsaeure

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 20 °C / Molecular sieve

2: hydrazine hydrate / methanol; chloroform / 1 h / 20 °C

3: sodium carbonate / ethyl acetate; water / 2 h / 0 °C

4: [Ru(C₅Me₅)(MeCN)₃](SbF₆)₂ / 10 h / 20 °C

5: lithium hydroxide / methanol; water / 5 h / 20 °C

With pyridine; [Ru(C₅Me₅)(MeCN)₃](SbF₆)₂; sodium carbonate; hydrazine hydrate; copper(l) chloride; lithium hydroxide; In methanol; chloroform; water; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1039/c5cc00354g