10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Base Information

Chemical Name:10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate
CAS No.:554450-42-9
Molecular Formula:C₄₃H₄₁O₅PS
Molecular Weight:700.835
Hs Code.:

Synonyms:10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Suppliers and Price of 10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

There total 7 articles about 10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-88-4
benzoyl chloride

: 554450-39-4
(1S)-10-(phenylsulfonyl)isobornyl (triphenylphosphoranylidene)acetate

: 554450-42-9
10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/S0040-4020(03)00248-5

Reference yield:

: 3144-16-9,61380-66-3
(1S)-10-camphorsulfonic acid

: 554450-42-9
10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Guidance literature:: Multi-step reaction with 6 steps

1: NaBJ₄

2: pyridine; TsCl

3: 94 percent / CH₂Cl₂ / 12 h / 20 °C

4: 87 percent / toluene / 12 h / Heating

5: 81 percent / NEt₃ / tetrahydrofuran / 12 h / 20 °C

With pyridine; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0040-4020(03)00248-5

Reference yield:

: 41348-33-8
(1S,5R,7R)-10,10-dimethyl-4-oxa-3-thiatricyclo[5.2.1.0^1,5]decane 3,3-dioxide

: 554450-42-9
10-phenylsulfonylisobornyl 3-oxo-3-phenyl-2-triphenylphosphoranylidenepropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / CH₂Cl₂ / 12 h / 20 °C

2: 87 percent / toluene / 12 h / Heating

3: 81 percent / NEt₃ / tetrahydrofuran / 12 h / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0040-4020(03)00248-5