1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

Base Information

Chemical Name:1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine
CAS No.:245411-52-3
Molecular Formula:C₂₀H₃₆N₄O₄P₂S₄
Molecular Weight:586.742
Hs Code.:

Synonyms:1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

Suppliers and Price of 1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

There total 1 articles about 1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 69674-00-6
diisopropoxythiophosphoryl isothiocyanate

: 95-54-5
1,2-diamino-benzene

: 245411-52-3
1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

Guidance literature:: In dichloromethane; for 1h;
DOI:10.1002/ejic.201000165

Reference yield: 89.0%

: 7681-65-4
copper(l) iodide

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 245411-52-3
1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

: [C₆H₄[Cu(CH₂P(C₆H₅)2)2(HNC(S)NP(S)(OC₃H₇)2)]2]

Guidance literature:: With KOH; In ethanol; dichloromethane; water; byproducts: KI; suspn. of ligand in aq. EtOH (0.5 mmol) treated with aq. EtOH soln. of KOH (1.1 mmol), mixt. of CuI (1.0 mmol) and P compd. (1.0 mmol) refluxed for 0.5 h in CH2Cl2, soln. added dropwise with vigorous stirring to EtOHsoln. of ligand, stirred for 1 h; filtered, concd., recrystd. (CH2Cl2/n-hexane=1/5), elem. anal.;
DOI:10.1002/ejic.201000165

Reference yield: 86.0%

: 24038-30-0
tetraphenylphosphonium bromide

: 245411-52-3
1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine

: C₂₀H₃₄N₄O₄P₂S₄^(2-)*2C₂₄H₂₀P⁽¹⁺⁾

Guidance literature:: 1,2-bis-N,N'-(diisopropoxythiophosphorylthiocarbamido)phenylenediamine; With sodium hydroxide; In ethanol; water;

tetraphenylphosphonium bromide; In ethanol; water; at 20 ℃;
DOI:10.1002/hc.20607