(2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide

Base Information

Chemical Name:(2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide
CAS No.:73718-47-5
Molecular Formula:C16H13N3OS2
Molecular Weight:327.431
Hs Code.:

Synonyms:BRN 1145278;(2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide;ACETIC ACID, (2-BENZOTHIAZOLYLTHIO)-, (PHENYLMETHYLENE)HYDRAZIDE;73718-47-5;C16H13N3OS2;C16-H13-N3-O-S2;STK870129;AKOS000606401;2-(1,3-benzothiazol-2-ylsulfanyl)-N'-[(E)-phenylmethylidene]acetohydrazide;2-(BENZOTHIAZOL-2-YLSULFANYL)-ACETIC ACID BENZYLIDENE-HYDRAZIDE

Suppliers and Price of (2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:327.05000439
Heavy Atom Count:22
Complexity:399

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=NNC(=O)CSC2=NC3=CC=CC=C3S2
Isomeric SMILES:C1=CC=C(C=C1)/C=N/NC(=O)CSC2=NC3=CC=CC=C3S2

Technology Process of (2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide

There total 4 articles about (2-Benzothiazolylthio)acetic acid (phenylmethylene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-52-7
benzaldehyde

: 24044-91-5
[(1,3-benzothiazol-2-ylthio)acetyl]hydrazine

: 73718-47-5
2-(1,3-benzothiazol-2-ylsulfanyl)-N'-[phenylmethylidene]acetohydrazide

Guidance literature:: In ethanol; for 8h; Heating;
DOI:10.1002/ardp.19953280614

Reference yield:

: 24044-88-0
ethyl 2-(benzo[d]thiazol-2-ylthio)acetate

: 73718-47-5
2-(1,3-benzothiazol-2-ylsulfanyl)-N'-[phenylmethylidene]acetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / H₂O; propan-2-ol; dioxane / 35 °C

2: 85 percent / dioxane / 2 h / Ambient temperature

With hydrazine hydrate; In 1,4-dioxane; water; isopropyl alcohol;
DOI:10.1007/BF01166343

Reference yield:

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 73718-47-5
2-(1,3-benzothiazol-2-ylsulfanyl)-N'-[phenylmethylidene]acetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / H₂O; propan-2-ol; dioxane / 1.5 h / 70 °C

2: hydrazine hydrate / H₂O; propan-2-ol; dioxane / 35 °C

3: 85 percent / dioxane / 2 h / Ambient temperature

With potassium hydroxide; hydrazine hydrate; In 1,4-dioxane; water; isopropyl alcohol;
DOI:10.1007/BF01166343