choladiene-1,4 one-3 oate-24 de methyle

Base Information

Chemical Name:choladiene-1,4 one-3 oate-24 de methyle
CAS No.:73409-98-0
Molecular Formula:C₂₅H₃₆O₃
Molecular Weight:384.559
Hs Code.:

Synonyms:choladiene-1,4 one-3 oate-24 de methyle

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Chemical Property of choladiene-1,4 one-3 oate-24 de methyle

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Technology Process of choladiene-1,4 one-3 oate-24 de methyle

There total 2 articles about choladiene-1,4 one-3 oate-24 de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1173-32-6
methyl 3-oxo-5β-cholan-24-oate

: 73409-98-0
choladiene-1,4 one-3 oate-24 de methyle

: 1452-33-1
methyl 3-oxo-4-cholenolate

: 91667-86-6
5β cholene-1, one-3, oate-24 de methyle

Guidance literature:: With diphenyl diselenide; 3-iodylbenzoic acid; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 1414953-61-9
C₂₅H₃₉BrO₃

: 99598-20-6
2,4-didromo-3-oxo lithicholic acid methyl ester

: 112018-64-1
(R)-4-((5S,8S,9S,10R,13R,14S,17R)-4-Bromo-10,13-dimethyl-3-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid methyl ester

: 73409-98-0
choladiene-1,4 one-3 oate-24 de methyle

: 1452-33-1
methyl 3-oxo-4-cholenolate

: 91667-86-6
5β cholene-1, one-3, oate-24 de methyle

Guidance literature:: With Li₂CO₃; lithium bromide; In N,N-dimethyl-formamide; Overall yield = 48 %;
DOI:10.1016/j.bmcl.2012.09.040

Reference yield: 55.0%

: 73409-98-0
choladiene-1,4 one-3 oate-24 de methyle

: 15074-03-0
(R)-methyl 4-((5S,8R,9S,10S,13R,14S,17R)-10,13-dimethyl-3-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoate

: 1173-32-6
methyl 3-oxo-5β-cholan-24-oate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h; under 735.5 Torr; Ambient temperature;
DOI:10.1016/0039-128X(89)90022-6