1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

Base Information

Chemical Name:1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide
CAS No.:135885-23-3
Molecular Formula:C₅H₁₀N₆S₂
Molecular Weight:218.307
Hs Code.:

Synonyms:1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

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Technology Process of 1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

There total 1 articles about 1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 92945-30-7
methyl (5-amino-3-methylthio-1,2,4-triazol-1-yl)dithiocarbonate

: 60-34-4
methylhydrazine

: 20184-94-5
N-methyl-hydrazinecarbodithioic acid methyl ester

: 135885-23-3
1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

: 45534-08-5
5-amino-3-methylthio-1,2,4-triazole

Guidance literature:: In methanol; for 20h; Ambient temperature;

Reference yield: 59.0%

: 103-72-0
phenyl isothiocyanate

: 135885-23-3
1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

: 1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methyl-N'-phenylthiocarbamoylcarbothiohydrazide

Guidance literature:: In N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 135885-23-3
1-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-N'-methylcarbothiohydrazide

: 2-(5-amino-3-methylthio-1H-1,2,4-triazol-1-yl)-5-phenylimino-4-methyl-4,5-dihydro-1,3,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / dimethylformamide / 1 h / Ambient temperature

2: 83 percent / dimethylformamide / 0.08 h / Heating

In N,N-dimethyl-formamide;