5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

Base Information

Chemical Name:5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole
CAS No.:901127-45-5
Molecular Formula:C₃₀H₃₄N₄O₆
Molecular Weight:546.623
Hs Code.:

Synonyms:5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

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Chemical Property of 5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

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Technology Process of 5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

There total 3 articles about 5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 303007-70-7
5,5'-bis(p-nitrobenzoyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

: 901127-45-5
5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 3h;
DOI:10.1039/b518340e

Reference yield:

: 7291-01-2
N,N-dimethyl-4-nitrobenzamide

: 901127-45-5
5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: POCl₃ / 24 h / 20 °C

1.2: various solvent(s) / 30 h / 20 °C

1.3: 86 percent / aq. K₂CO₃ / various solvent(s) / 3 h / Heating

2.1: 98 percent / NaBH₄ / tetrahydrofuran; methanol / 3 h / 20 °C

With sodium tetrahydroborate; trichlorophosphate; In tetrahydrofuran; methanol;
DOI:10.1039/b518340e

Reference yield:

: 152172-77-5
3,4,3',4'-tetraethyl-1H,1H'-[2,2']-bipyrrole

: 901127-45-5
5,5'-bis(p-nitrophenyl(hydroxy)methyl)-3,3',4,4'-tetraethyl-2,2'-bipyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: POCl₃ / 24 h / 20 °C

1.2: various solvent(s) / 30 h / 20 °C

1.3: 86 percent / aq. K₂CO₃ / various solvent(s) / 3 h / Heating

2.1: 98 percent / NaBH₄ / tetrahydrofuran; methanol / 3 h / 20 °C

With sodium tetrahydroborate; trichlorophosphate; In tetrahydrofuran; methanol;
DOI:10.1039/b518340e