N,N-dimethyl-4-nitrobenzamide

Base Information

• Chemical Name: N,N-dimethyl-4-nitrobenzamide
• CAS No.: 7291-01-2
• Molecular Formula: C9H10N2O3
• Molecular Weight: 194.19
• Hs Code.: 2924299090
• Mol file: 7291-01-2.mol

Synonyms:N,N-dimethyl-p-nitrobenzoamide;4-nitro-N,N-dimethylbenzamide;N,N-dimethyl(4-nitrophenyl)carboxamide;N,N-dimethyl-p-nitrobenzamide;Benzamide,N,N-dimethyl-p-nitro;N,N-dimethyl 4-nitrobenzamide;Benzamide,N,N-dimethyl-4-nitro;

Chemical Property of N,N-dimethyl-4-nitrobenzamide

Chemical Property:

• Vapor Pressure: 1.43E-05mmHg at 25°C
• Melting Point: 93-95°C
• Boiling Point: 366.8°C at 760 mmHg
• Flash Point: 175.6°C
• PSA: 66.13000
• Density: 1.24g/cm³
• LogP: 1.81980
• Storage Temp.: Room Temperature
• Solubility.: Chloroform, Methanol (Slightly, Heated)

Purity/Quality:

99%, ^*data from raw suppliers

N,N-Dimethyl-4-nitrobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of N,N-dimethyl-4-nitrobenzamide

There total 36 articles about N,N-dimethyl-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 4-nitro-benzoic acid (62-23-7) → N,N-dimethyl-4-nitrobenzamide (7291-01-2)

Guidance literature:

With sulfur trioxide pyridine complex; at 160 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1246/cl.171216

Reference yield: 99.0%

N,N-dimethylammonium chloride (506-59-2) + 4-nitro-benzoic acid (62-23-7) → N,N-dimethyl-4-nitrobenzamide (7291-01-2)

Guidance literature:

With ethylene dichloride hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield: 97.0%

dimethyl amine (124-40-3) + 4-nitro-benzoic acid (62-23-7) → N,N-dimethyl-4-nitrobenzamide (7291-01-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2005.10.068

upstream raw materials:

4-nitro-benzoyl chloride

dimethyl amine

N,N-dimethylsulfamide

4-nitro-benzoic acid

Downstream raw materials:

4-amino-N,N-dimethylbenzamide

4,4'-azoxy-di-benzoic acid bis-dimethylamide

4-(N,N-dimethylaminomethyl)nitrobenzene

N-(chloro(4-nitrophenyl)methylene)-N-methylmethanaminium chloride

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