p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

Base Information

Chemical Name:p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate
CAS No.:197963-40-9
Molecular Formula:C₃₀H₂₆ClNO₆
Molecular Weight:531.993
Hs Code.:

Synonyms:p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

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Chemical Property of p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

Chemical Property:

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Technology Process of p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

There total 7 articles about p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 178313-89-8
p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-hydroxymethyl]phenyl}-propionate

: 197963-40-9
p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

Guidance literature:: With acetyl chloride; for 3h; Heating;
DOI:10.1016/0040-4020(96)00337-7

Reference yield:

: 66885-68-5
(E)-p-formylcinnamic acid

: 197963-40-9
p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 5percent Pd/C

2: 41 percent / glacial AcOH, conc. H₂SO₄ / Ambient temperature

3: 99 percent / N,N'-dicyclohexylcarbodiimide, pyridine / dioxane / Ambient temperature

4: 50 percent / glacial AcOH, PbO₂

5: AcCl / 3 h / Heating

With pyridine; sulfuric acid; hydrogen; lead dioxide; acetic acid; acetyl chloride; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1016/0040-4020(96)00337-7

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 197963-40-9
p-Nitrophenyl-3-{4-[bis-(4-methoxyphenyl)-chlormethyl]-phenyl}-propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / N,N'-dicyclohexylcarbodiimide, pyridine / dioxane / Ambient temperature

2: 50 percent / glacial AcOH, PbO₂

3: AcCl / 3 h / Heating

With pyridine; lead dioxide; acetic acid; acetyl chloride; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1016/0040-4020(96)00337-7