C₁₄H₂₃O₄P

Base Information

Chemical Name:C₁₄H₂₃O₄P
CAS No.:873799-83-8
Molecular Formula:C₁₄H₂₃O₄P
Molecular Weight:286.308
Hs Code.:

C<sub>14</sub>H<sub>23</sub>O<sub>4</sub>P

Synonyms:C₁₄H₂₃O₄P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₃O₄P

Chemical Property:

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Technology Process of C₁₄H₂₃O₄P

There total 2 articles about C₁₄H₂₃O₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 589-57-1
diethyl phosphorylchloridite

: 5426-78-8
acetaldehyde phenyl ethyl acetal

: 873799-83-8
C₁₄H₂₃O₄P

Guidance literature:: acetaldehyde phenyl ethyl acetal; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; cyclohexane; at -60 - 20 ℃;

diethyl phosphorylchloridite; In diethyl ether; hexane; cyclohexane; at -70 - 20 ℃; for 16h;
DOI:10.1021/ja046901f

Reference yield:

: 108-95-2,27073-41-2
phenol

: 873799-83-8
C₁₄H₂₃O₄P

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 2.5 h

2.1: n-BuLi; TMEDA / diethyl ether; hexane; cyclohexane / -60 - 20 °C

2.2: 72 percent / diethyl ether; hexane; cyclohexane / 16 h / -70 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In diethyl ether; hexane; dichloromethane; cyclohexane;
DOI:10.1021/ja046901f