14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

Base Information

Chemical Name:14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin
CAS No.:1430847-70-3
Molecular Formula:C₃₄H₅₀N₂O₅S
Molecular Weight:598.847
Hs Code.:

Synonyms:14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

Chemical Property:

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Technology Process of 14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

There total 4 articles about 14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 133787-61-8
14-O-[(1-amino-2-methylpropane-2-yl)thioacetyl]mutilin

: 4257-87-8
N-(2-methylphenyl)-2,2,2,-trichloroacetamide

: 1430847-70-3
14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 80 ℃;
DOI:10.2174/1570180811310030005

Reference yield:

: 95-53-4
o-toluidine

: 1430847-70-3
14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride / 110 °C

2: potassium carbonate / dimethyl sulfoxide / 80 °C

With potassium carbonate; phosphorus trichloride; In dimethyl sulfoxide;
DOI:10.2174/1570180811310030005

Reference yield:

: pleuromutilin

: 1430847-70-3
14-O-{1-[(2-methylphenyl)ureido]-2-methylpropan-2-ylthioacetyl}mutilin

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; pyridine / 1,2-dichloro-ethane / 20 h / 10 - 15 °C

2.1: ethanol; sodium / 0.5 h / -5 °C

2.2: 2 h / 0 - 5 °C

3.1: potassium carbonate / dimethyl sulfoxide / 80 °C

With pyridine; ethanol; sodium; potassium carbonate; triethylamine; In dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.2174/1570180811310030005