benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

Base Information

Chemical Name:benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate
CAS No.:1369963-18-7
Molecular Formula:C₂₇H₄₁NO₅SSi
Molecular Weight:519.778
Hs Code.:

Synonyms:benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

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Chemical Property of benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

Chemical Property:

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Technology Process of benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

There total 3 articles about benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(4-isopropylphenyl)methanesulfonamide

: 1208982-25-5
benzyl 4-(tert-butyldimethylsiloxy)-2-hydroxybutanoate

: 1369963-18-7
benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 0.5h; Cooling with ice; Inert atmosphere;

Reference yield:

: 100-39-0
benzyl bromide

: 1369963-18-7
benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / methanol / 1 h / 20 °C

1.2: 20 °C

2.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / Cooling with ice; Inert atmosphere

With dmap; di-isopropyl azodicarboxylate; water; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1369962-91-3
benzyl 2,4-dihydroxybutanoate

: 1369963-18-7
benzyl O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)-N-[4-(propan-2-yl)phenyl]homoserinate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / Cooling with ice; Inert atmosphere

With dmap; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;