4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

Base Information

Chemical Name:4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate
CAS No.:289903-56-6
Molecular Formula:C₁₁H₁₂N₄O₂S
Molecular Weight:264.308
Hs Code.:

Synonyms:4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

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Chemical Property of 4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

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Technology Process of 4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

There total 5 articles about 4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 102368-13-8
1,1'-Thiocarbonyldi-2(1H)-pyridone

: 4-(2-Azidoethoxy)-3-methoxy-benzylamine Trifluoroacetate

: 289903-56-6
4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 7149-10-2
vanillylamine hydrochloride

: 289903-56-6
4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / triethylamine / dioxane; H₂O / 24 h / 20 °C

2: 84 percent / tetrabutylammonium hydroxide; potassium hydroxide / H₂O / 2 h / 50 °C

3: 98 percent / sodium azide / dimethylformamide / 8 h / 100 °C

4: CH₂Cl₂ / 1 h / 20 °C

5: 270 mg / triethylamine / dimethylformamide / 3 h / 20 °C

With potassium hydroxide; sodium azide; tetra(n-butyl)ammonium hydroxide; triethylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00387-X

Reference yield:

: 130972-89-3
(4-hydroxy-3-methoxybenzyl)carbamic acid tert-butyl ester

: 289903-56-6
4-(2-azidoethoxy)-3-methoxybenzylisothiocyanate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / tetrabutylammonium hydroxide; potassium hydroxide / H₂O / 2 h / 50 °C

2: 98 percent / sodium azide / dimethylformamide / 8 h / 100 °C

3: CH₂Cl₂ / 1 h / 20 °C

4: 270 mg / triethylamine / dimethylformamide / 3 h / 20 °C

With potassium hydroxide; sodium azide; tetra(n-butyl)ammonium hydroxide; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00387-X