(RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

Base Information

Chemical Name:(RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide
CAS No.:374793-76-7
Molecular Formula:C₂₄H₂₃F₆NO
Molecular Weight:455.443
Hs Code.:

Synonyms:(RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

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Technology Process of (RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

There total 1 articles about (RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 374791-10-3
(RS)-α-methyl-N-[4-oxo-1-phenylcyclohexyl]-3,5-bis(trifluoromethyl)benzeneacetamide

: 374793-76-7
(RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

(RS)-α-methyl-N-[4-oxo-1-phenylcyclohexyl]-3,5-bis(trifluoromethyl)benzeneacetamide; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Heating / reflux;

Reference yield: 40.0%

: 374793-76-7
(RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

: cis-(RS) and trans-(RS)-α-methyl-N-(4-hydroxymethyl-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl)benzeneacetamide

Guidance literature:: (RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide; With borane; In tetrahydrofuran; at 20 ℃;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 3h;

Reference yield: 21.0%

: 374793-76-7
(RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide

: cis (RS)-α-methyl-N-(6-phenyl-1-oxaspiro[2.5]oct-6-yl)-3,5-bis(trifluoromethyl)benzeneacetamide

Guidance literature:: (RS)-α-methyl-N-4-(4-methylene-1-phenylcyclohexyl)-3,5-bis(trifluoromethyl) benzeneacetamide; With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 2h;

With sodium hydrogensulfide; sodium hydrogencarbonate; In chloroform; water; at 20 ℃; for 1h;