C₂₀H₂₈N₂O₃

Base Information

Chemical Name:C₂₀H₂₈N₂O₃
CAS No.:930117-90-1
Molecular Formula:C₂₀H₂₈N₂O₃
Molecular Weight:344.454
Hs Code.:

C<sub>20</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₀H₂₈N₂O₃

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Chemical Property of C₂₀H₂₈N₂O₃

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Technology Process of C₂₀H₂₈N₂O₃

There total 4 articles about C₂₀H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 930117-84-3
methyl (Z)-2-(acetylamino)-3-[4-(hydroxymethyl)phenyl]propenoate

: cis-2,6-dimethylpiperidine

: 930117-90-1
C₂₀H₂₈N₂O₃

Guidance literature:: methyl (Z)-2-(acetylamino)-3-[4-(hydroxymethyl)phenyl]propenoate; With N-ethyl-N,N-diisopropylamine; Methanesulfonic anhydride; In dichloromethane;

cis-2,6-dimethylpiperidine; In dichloromethane;
DOI:10.1021/op200129m

Reference yield:

: 14720-70-8
1,4-bis(hydroxymethyl)benzene diacetate

: 930117-90-1
C₂₀H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethyl acetate / 18 h / 93 - 95 °C

2.1: potassium carbonate / 1.75 h

2.2: Dowex 50WX-8-200 ion-exchange resin / pH 6 - 7

3.1: N-ethyl-N,N-diisopropylamine; Methanesulfonic anhydride / dichloromethane

With potassium carbonate; N-ethyl-N,N-diisopropylamine; Methanesulfonic anhydride; In dichloromethane; ethyl acetate;
DOI:10.1021/op200129m

Reference yield:

: 623-27-8
terephthalaldehyde,

: 930117-90-1
C₂₀H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; water / 2.33 h / 30 °C

2.1: sodium acetate; acetic anhydride / ethyl acetate / Reflux

3.1: potassium carbonate / 1.75 h

3.2: Dowex 50WX-8-200 ion-exchange resin / pH 6 - 7

4.1: N-ethyl-N,N-diisopropylamine; Methanesulfonic anhydride / dichloromethane

With sodium tetrahydroborate; sodium acetate; acetic anhydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; Methanesulfonic anhydride; In tetrahydrofuran; dichloromethane; water; ethyl acetate; 2.1: Erlenmeyer-Plochl azlactone and amino acid synthesis;
DOI:10.1021/op200129m