(C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

Base Information

Chemical Name:(C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride
CAS No.:856704-85-3
Molecular Formula:C₃₂H₃₂P₂Ru
Molecular Weight:579.624
Hs Code.:

(C<sub>5</sub>H<sub>4</sub>Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

Synonyms:(C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

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Chemical Property of (C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

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Technology Process of (C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

There total 1 articles about (C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 67-56-1
methanol

: Ru(η5-CH3C5H4)Cl(dppe)

: 856704-85-3
(C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

Guidance literature:: With Na; In methanol; (N2), Na added to suspn. of Ru complex in CH3OH, boiled for 3 h; cooled to room temp., washed (CH3OH), dried (vac.), elem. anal.;
DOI:10.1021/ja0506861

Reference yield: 74.0%

: 856704-85-3
(C₅H₄Me) [1,2-bis(diphenylphosphino)ethane]ruthenium hydride

: 67969-83-9
tetrafluoroboric acid dimethyl ether complex

: (C5H4Me)(1,2-bis(diphenylphosphino)ethane)ruthenium (η2-dihydrogen) BF4

Guidance literature:: In diethyl ether; Ru complex in Et2O treated with HBF4*OMe2 in Et2O, stirred for 30 min; filtered, washed (Et2O), dried (vac.), elem. anal.;
DOI:10.1021/ja0506861