t-butylchloro{mesityl(trimethylsilyl)amino}borane

Base Information

Chemical Name:t-butylchloro{mesityl(trimethylsilyl)amino}borane
CAS No.:118331-69-4
Molecular Formula:C₁₆H₂₉BClNSi
Molecular Weight:309.762
Hs Code.:

Synonyms:t-butylchloro{mesityl(trimethylsilyl)amino}borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of t-butylchloro{mesityl(trimethylsilyl)amino}borane

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Technology Process of t-butylchloro{mesityl(trimethylsilyl)amino}borane

There total 1 articles about t-butylchloro{mesityl(trimethylsilyl)amino}borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 109-72-8,29786-93-4
n-butyllithium

: 76873-78-4
tert-butyldichloroborane

: 69563-04-8
N-(trimethylsilyl)-2,4,6-trimethylaniline

: 118331-69-4
t-butylchloro{mesityl(trimethylsilyl)amino}borane

Guidance literature:: In diethyl ether; hexane; n-BuLi in hexane added to Mes(SiMe3)NH in Et2O at 0°C; stirring for 1 h at room temp.; mixt. added to a soln. of t-BuBCl2 in hexane at -78°C; stirring at room temp. for 2 h; soln. filtered; vac. distn.; elem. anal.;

Reference yield: 75.0%

: 118331-69-4
t-butylchloro{mesityl(trimethylsilyl)amino}borane

: 75-77-4
chloro-trimethyl-silane

: 118331-72-9
t-butyl(mesitylimino)borane

Guidance literature:: In neat (no solvent); thermal decompn. of t-BuBClN(Mes)SiMe3 575°C and 0.005 Torr; products condensed at -196°C; mixt. liquefies at ca. -55°C; Me3SiCl removed at -45°C in vac.;

Reference yield: 59.0%

: 118331-69-4
t-butylchloro{mesityl(trimethylsilyl)amino}borane

: 118346-12-6
2,4-di-t-butyl-1,3-dimesityl-1,3,2,4-diazadiboretidine

Guidance literature:: In hexane; products of the thermal decompn. of t-BuBClN(Mes)SiMe3 at 575°C and 0.005 Torr are dissolved in pentane at -78°C; soln. warmed up to room temp. and stirred for 12 h; pptd. diazadiboretidine filtered, washed with few pentane, dried in vac.; elem. anal.;