(2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

Base Information

Chemical Name:(2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester
CAS No.:908366-29-0
Molecular Formula:C₂₂H₂₉NO₇
Molecular Weight:419.475
Hs Code.:

Synonyms:(2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

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Chemical Property of (2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

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Technology Process of (2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

There total 11 articles about (2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 333-27-7
methyl trifluoromethanesulfonate

: 908365-91-3
(2S,5S)-N-benzoyl-5-(di(ethoxycarbonyl)methyl)-pyrrolidine-2-carboxylic acid ethyl ester

: 908366-29-0
(2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

Guidance literature:: (2S,5S)-N-benzoyl-5-(di(ethoxycarbonyl)methyl)-pyrrolidine-2-carboxylic acid ethyl ester; With potassium hydride; In diethyl ether; at 20 ℃; for 2.5h;

methyl trifluoromethanesulfonate; In diethyl ether; at -40 - 20 ℃; for 2.5h; Further stages.;
DOI:10.1039/b604183c

Reference yield: 25.0%

: 675588-13-3
(2S,5R)-N-benzoyl-5-(di(ethoxycarbonyl)methyl)-pyrrolidine-2-carboxylic acid ethyl ester

: 74-88-4
methyl iodide

: 908366-29-0
(2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

Guidance literature:: (2S,5R)-N-benzoyl-5-(di(ethoxycarbonyl)methyl)-pyrrolidine-2-carboxylic acid ethyl ester; With sodium hydride; In N,N-dimethyl-formamide;

methyl iodide; In N,N-dimethyl-formamide; Further stages.;
DOI:10.1039/b303789d

Reference yield: 25.0%

: 908365-91-3
(2S,5S)-N-benzoyl-5-(di(ethoxycarbonyl)methyl)-pyrrolidine-2-carboxylic acid ethyl ester

: 74-88-4
methyl iodide

: 908366-29-0
(2S,5S)-N-benzoyl-5-(1,1-di(ethoxycarbonyl)ethyl)-pyrrolidine-2-carboxylic acid ethyl ester

Guidance literature:: (2S,5S)-N-benzoyl-5-(di(ethoxycarbonyl)methyl)-pyrrolidine-2-carboxylic acid ethyl ester; With sodium hydride; In N,N-dimethyl-formamide;

methyl iodide; In N,N-dimethyl-formamide; Further stages.;
DOI:10.1039/b303789d