[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄

Base Information

• Chemical Name: [(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄
• CAS No.: 954149-66-7
• Molecular Formula: BF₄*C₂₇H₂₆FeN₂PS
• Molecular Weight: 584.208

Synonyms:[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄

Chemical Property of [(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄

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Technology Process of [(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄

There total 1 articles about [(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2S)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1-methyl-1H-imidazole (616-47-7) + tetrafluoroboric acid + [1'-(diphenylthiophosphanyl)ferrocen-1-yl]methanol (954149-64-5) → [(C5H4P(C6H5)2S)Fe(C5H4CH2N2(CH3)C3H3)](1+)*BF4(1-)=[(C5H4P(C6H5)2S)Fe(C5H4CH2N2(CH3)C3H3)]BF4 (954149-66-7)

Guidance literature:

In diethyl ether; dichloromethane; Ar, to a soln. of Fe compd. (CH2Cl2) quickly added acid (diethyl ether, room temp.), imidazole deriv.; washed (aq. HCl, water, aq. NaHCO3, water), dried (MgSO4), filtered, concd. (vac.), repptd. (CH2Cl2/diethyl ether), ppt. filtered, washed (diethyl ether), dried (vac.); elem. anal., XRD;

DOI:10.1002/ejic.200601193

Reference yield: 100.0%

[(C5H4P(C6H5)2S)Fe(C5H4CH2N2(CH3)C3H3)](1+)*BF4(1-)=[(C5H4P(C6H5)2S)Fe(C5H4CH2N2(CH3)C3H3)]BF4 (954149-66-7) → [(C5H4P(C6H5)2)Fe(C5H4CH2N2(CH3)C3H3)](1+)*BF4(1-)=[(C5H4P(C6H5)2)Fe(C5H4CH2N2(CH3)C3H3)]BF4 (954149-75-8)

Guidance literature:

nickel; In acetonitrile; at room temp. or at 80°C;

DOI:10.1002/ejic.200601193

upstream raw materials:

1-methyl-1H-imidazole

[1'-(diphenylthiophosphanyl)ferrocen-1-yl]methanol

Downstream raw materials:

[(C₅H₄P(C₆H₅)2)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]⁽¹⁺⁾*BF₄^(1-)=[(C₅H₄P(C₆H₅)2)Fe(C₅H₄CH₂N₂(CH₃)C₃H₃)]BF₄

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