N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide

Base Information

• Chemical Name: N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide
• CAS No.: 1257660-76-6
• Molecular Formula: C₂₇H₃₀N₂O₇S₃
• Molecular Weight: 590.742
• Mol file: 1257660-76-6.mol

Synonyms:N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide

Chemical Property of N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide

There total 2 articles about N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

1-hexene (592-41-6,25067-06-5) + di(4-tosyl)amine (3695-00-9) + saccharin (81-07-2) → N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide (1257660-76-6)

Guidance literature:

With bis(benzonitrile)palladium(II) dichloride; bis(tertbutylcarbonyloxy)iodobenzene; In dichloromethane; at 20 ℃; for 16h; regioselective reaction;

DOI:10.1002/anie.201003653

Reference yield: 73.0%

→ N-(2-(1,1-dioxido-3-oxobenzo[d]isothiazol-2(3H)-yl)hexyl)-4-methyl-N-tosylbenzenesulfonamide (1257660-76-6)

Guidance literature:

upstream raw materials:

1-hexene

di(4-tosyl)amine

saccharin