(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

Base Information

Chemical Name:(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine
CAS No.:625114-90-1
Molecular Formula:C₁₁H₁₂F₃NO
Molecular Weight:231.218
Hs Code.:

Synonyms:(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

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Chemical Property of (1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

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Technology Process of (1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

There total 1 articles about (1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-90-1
2,2,2-Trifluoroacetaldehyde

: 64715-85-1,91298-74-7,127180-88-5
(R)-2-methoxy-1-phenylethylamine

: 625114-90-1
(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

Guidance literature:: In toluene; Heating;
DOI:10.3987/COM-02-S(M)32

Reference yield: 95.0%

: 1066-54-2
trimethylsilylacetylene

: 625114-90-1
(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

: 850786-06-0
(-)-[(R)-2-methoxy-1-phenylethyl][(R)-1-(trifluoromethyl)-3-(trimethylsilyl)prop-2-ynyl]amine

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In hexane; toluene; at -78 ℃; for 0.5h;

(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine; In hexane; toluene; at -78 - 20 ℃; for 15h;
DOI:10.1002/ejoc.200701090

Reference yield: 90.0%

: 536-74-3
phenylacetylene

: 625114-90-1
(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine

: 850786-08-2
(-)-[(R)-2-methoxy-1-phenylethyl][(R)-3-phenyl-1-(trifluoromethyl)prop-2-ynyl]amine

Guidance literature:: phenylacetylene; With n-butyllithium; In hexane; toluene; at -78 ℃; for 0.5h;

(1R)-2-methoxy-1-phenyl-N-[(E)-2,2,2-trifluoroethylidene]-1-ethaneamine; In hexane; toluene; at -78 - 20 ℃; for 15h;
DOI:10.1002/ejoc.200701090