1,10-Bis(1-hydroxy-2-naphthyl)decane-1,10-dione

Base Information

• Chemical Name: 1,10-Bis(1-hydroxy-2-naphthyl)decane-1,10-dione
• CAS No.: 13379-63-0
• Molecular Formula: C₃₀H₃₀O₄
• Molecular Weight: 454.566
• Hs Code.: 2914501900
• European Community (EC) Number: 654-983-1
• NSC Number: 120641
• DSSTox Substance ID: DTXSID10298113
• Wikidata: Q82039727
• Mol file: 13379-63-0.mol

Synonyms:13379-63-0;1,10-bis(1-hydroxy-2-naphthyl)decane-1,10-dione;1,10-bis(1-hydroxynaphthalen-2-yl)decane-1,10-dione;1,10-Bis-(1-Hydroxy-2-Naphthyl)-1,10-Decanedione;1,10-Decanedione,1,10-bis(1-hydroxy-2-naphthyl)- (6CI,8CI);NSC120641;DTXSID10298113;AKOS022180752;NSC-120641

Chemical Property of 1,10-Bis(1-hydroxy-2-naphthyl)decane-1,10-dione

Chemical Property:

• Vapor Pressure: 2.38E-18mmHg at 25°C
• Boiling Point: 666°C at 760 mmHg
• Flash Point: 370.6°C
• PSA: 74.60000
• Density: 1.204g/cm³
• LogP: 7.59060
• XLogP3: 8.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 11
• Exact Mass: 454.21440943
• Heavy Atom Count: 34
• Complexity: 604

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,10-Bis-(1-hydroxy-2-Naphthyl)-1,10-decanedione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC(=C2O)C(=O)CCCCCCCCC(=O)C3=C(C4=CC=CC=C4C=C3)O

Technology Process of 1,10-Bis(1-hydroxy-2-naphthyl)decane-1,10-dione

There total 3 articles about 1,10-Bis(1-hydroxy-2-naphthyl)decane-1,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,10-decanedioic acid (111-20-6,26776-29-4) + α-naphthol (90-15-3) → 1,10-Di-(1-hydroxy-2-naphthyl)-decan-1,10-dion (13379-63-0)

Guidance literature:

With boron trifluoride diethyl etherate;

DOI:10.1021/ja01158a091

Reference yield:

sebacoyl chloride (111-19-3) + α-naphthol (90-15-3) → 1,10-Di-(1-hydroxy-2-naphthyl)-decan-1,10-dion (13379-63-0) + 1,10-bis-(4-hydroxy-[1]naphthyl)-decane-1,10-dione (116027-78-2)

Guidance literature:

With aluminium trichloride;

Reference yield:

→ 1,10-Di-(1-hydroxy-2-naphthyl)-decan-1,10-dion (13379-63-0)

Guidance literature:

Sebacinsaeure, α-Naphthol, BF3-Anisol;

upstream raw materials:

1,10-decanedioic acid

α-naphthol

sebacoyl chloride