5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene

Base Information

• Chemical Name: 5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene
• CAS No.: 97452-60-3
• Molecular Formula: C₂₇H₄₂O₂
• Molecular Weight: 398.629

Synonyms:5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene

Chemical Property of 5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene

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Technology Process of 5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene

There total 2 articles about 5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methanol (67-56-1) + HU 219 (97452-63-6) → 5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene (97452-60-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

DOI:10.1039/b416943c

Reference yield: 24.0%

(1S,4R)-p-mentha-2,8-dien-1-ol (22972-51-6) + 1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene (60526-81-0) → 5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene (97452-60-3)

Guidance literature:

With aluminum oxide; boron trifluoride diethyl etherate; In dichloromethane; at 40 - 41 ℃; for 0.00277778h;

DOI:10.1016/S0040-4039(00)98518-6

Reference yield: 70.0%

5-(1,1-Dimethyl-heptyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-1,3-dimethoxy-benzene (97452-60-3) → (1S,4R,5R,6R)-5-[4-(1,1-Dimethyl-heptyl)-2,6-dimethoxy-phenyl]-4-isopropenyl-1-methyl-7-oxa-bicyclo[4.1.0]heptane (380495-62-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1039/b416943c

upstream raw materials:

(1S,4R)-p-mentha-2,8-dien-1-ol

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

methanol

HU 219

Downstream raw materials:

(1S,4R,5R,6R)-5-[4-(1,1-Dimethyl-heptyl)-2,6-dimethoxy-phenyl]-4-isopropenyl-1-methyl-7-oxa-bicyclo[4.1.0]heptane

{(3R,4R)-3-[4-(1,1-Dimethyl-heptyl)-2,6-dimethoxy-phenyl]-4-isopropenyl-cyclohex-1-enyl}-methanol

2-((1R,6R)-3-Bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-(1,1-dimethyl-heptyl)-1,3-dimethoxy-benzene

(3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dimethoxyphenyl]-2-hydroxy-4-isopropenyl-1-methylenecyclohexane

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