bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

Base Information

Chemical Name:bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)
CAS No.:98687-67-3
Molecular Formula:C₃₅H₃₅Au₂BrP₂
Molecular Weight:991.447
Hs Code.:

Synonyms:bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

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Chemical Property of bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

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Technology Process of bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

There total 3 articles about bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: [Au2(μ-(CH2)2PPh2)2]

: 100-39-0
benzyl bromide

: 98687-67-3
bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

Guidance literature:: In 1,2-dichloro-ethane; The soln. of complex in 1,2-dichloroethane was filtered, benzyl bromidewas added to the stirred soln., 2 h (N2 atm.);; concd., cooled to -18°C for 20 h, filtered, ppt. was rinsed withEt2O, dried;;
DOI:10.1021/ja00310a028

Reference yield:

: 89462-48-6
bis[μ-(diphenyldimethylenephosphoranyl-C,C)]bromomethyldigold(II)(Au-Au)

: 98687-67-3
bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent)

2: 1,2-dichloro-ethane

In 1,2-dichloro-ethane;
DOI:10.1021/ja00310a028

Reference yield:

: CH₃Au(CH₂P(C₆H₅)2CH₂)2AuI

: 98687-67-3
bis[μ-(diphenyldimethylenephosphoranyl-C,C)]benzylbromodigold(II)(Au-Au)

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent)

2: 1,2-dichloro-ethane

In 1,2-dichloro-ethane;
DOI:10.1021/ja00310a028