benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

Base Information

Chemical Name:benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside
CAS No.:114218-05-2
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:266.306
Hs Code.:

Synonyms:benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

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Chemical Property of benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

Chemical Property:

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Technology Process of benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

There total 5 articles about benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 114244-38-1
benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

: 114218-05-2
benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

Guidance literature:: With tributyltin deuteride; In toluene; for 23h; Heating;
DOI:10.1016/S0040-4020(01)86822-8

Reference yield:

: 28070-06-6
benzyl-3,4-O-isopropylidene-β-D-erythro-pentoribopyranosid-2-ulose

: 114218-05-2
benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / lithium aluminium deuteride / tetrahydrofuran / 1.) 15 min., 0 deg C, 2.) 3 h. room temp.

3: 79 percent / tributyltin deuteride / toluene / 23 h / Heating

With lithium aluminium deuteride; tributyltin deuteride; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)86822-8

Reference yield:

: 114218-04-1
benzyl 3,4-isopropylidene-2(R)-deuterio-β-D-erythro-pentopyranoside

: 114218-05-2
benzyl 3,4-isopropylidene-2-deoxy-2,2'-dideuterio-erythro-pentopyranoside

Guidance literature:: Multi-step reaction with 2 steps

2: 79 percent / tributyltin deuteride / toluene / 23 h / Heating

With tributyltin deuteride; In toluene;
DOI:10.1016/S0040-4020(01)86822-8