(S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester

Base Information

• Chemical Name: (S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester
• CAS No.: 73995-61-6
• Molecular Formula: C₁₅H₂₁NO₃
• Molecular Weight: 263.337

Synonyms:(S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester

Chemical Property of (S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester

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Technology Process of (S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester

There total 1 articles about (S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl (L)-leucinate hydrochloride (7517-19-3) + 4-methoxy-benzaldehyde (123-11-5) → (S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester (73995-61-6)

Guidance literature:

With sodium carbonate; In methanol; for 12h; Ambient temperature;

DOI:10.1055/s-1987-28189

Reference yield:

(S)-2-{[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester (73995-61-6) → (-)-2-((4-methoxybenzyl)amino)-4-methylpentanoic acid methyl ester

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃;

DOI:10.1021/co300015k

Reference yield:

(S)-2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-4-methyl-pentanoic acid methyl ester (73995-61-6) → (S)-2-[(2R,3S)-3-(4-Methoxy-phenyl)-oxaziridin-2-yl]-4-methyl-pentanoic acid methyl ester + (S)-2-[(2R,3R)-3-(4-Methoxy-phenyl)-oxaziridin-2-yl]-4-methyl-pentanoic acid methyl ester + (S)-2-[(2S,3S)-3-(4-Methoxy-phenyl)-oxaziridin-2-yl]-4-methyl-pentanoic acid methyl ester + (S)-2-[(2S,3R)-3-(4-Methoxy-phenyl)-oxaziridin-2-yl]-4-methyl-pentanoic acid methyl ester

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -40 ℃; for 23h;

DOI:10.1021/jo051890+

upstream raw materials:

methyl (L)-leucinate hydrochloride

4-methoxy-benzaldehyde

Downstream raw materials:

(S)-2-[3-(4-Methoxy-phenyl)-oxaziridin-2-yl]-4-methyl-pentanoic acid methyl ester

N-(2-Boc-amino-3-phenylpropyliden)-L-leucin-N-oxid-methylester

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