Technology Process of 4-benzyloxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoic acid
There total 7 articles about 4-benzyloxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
dimethyl sulfoxide;
for 14h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 83 percent / K2CO3 / dimethylformamide / 48 h / Ambient temperature
2: 85-90percent m-chloroperoxybenzoic acid / CH2Cl2 / 2 h / Ambient temperature
3: 84 percent / K2CO3 / acetone / 22 h / Heating
4: 85 percent / H2 / 10percent Pd/C / ethyl acetate / 12 h / Ambient temperature
5: 61 percent / trifluoroacetic anhydride / toluene / 24 h / Ambient temperature
6: 84 percent / K2CO3 / dimethylsulfoxide / 14 h / Ambient temperature
With
hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride;
palladium on activated charcoal;
In
dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85-90percent m-chloroperoxybenzoic acid / CH2Cl2 / 2 h / Ambient temperature
2: 84 percent / K2CO3 / acetone / 22 h / Heating
3: 85 percent / H2 / 10percent Pd/C / ethyl acetate / 12 h / Ambient temperature
4: 61 percent / trifluoroacetic anhydride / toluene / 24 h / Ambient temperature
5: 84 percent / K2CO3 / dimethylsulfoxide / 14 h / Ambient temperature
With
hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride;
palladium on activated charcoal;
In
dichloromethane; dimethyl sulfoxide; ethyl acetate; acetone; toluene;
