C₁₆H₁₉ClO₇

Base Information

• Chemical Name: C₁₆H₁₉ClO₇
• CAS No.: 942044-36-2
• Molecular Formula: C₁₆H₁₉ClO₇
• Molecular Weight: 358.776
• Mol file: 942044-36-2.mol

Synonyms:C₁₆H₁₉ClO₇

Chemical Property of C₁₆H₁₉ClO₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₆H₁₉ClO₇

There total 1 articles about C₁₆H₁₉ClO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

methyl 2,3,4,6-tetrakis-O-trimethylsilyl-α-D-glucopyranoside (2641-79-4) + acetic anhydride (108-24-7) + 4-chlorobenzaldehyde (104-88-1) + benzaldehyde (100-52-7) + 4-bromo-benzaldehyde (1122-91-4) + benzoic acid anhydride (93-97-0) → C16H19ClO7 (942044-36-2) + C21H21ClO7 (942044-37-3) + methyl 2-O-acetyl-4,6-O-benzylidene-α-D-glucopyranoside (2774-23-4,20750-02-1,25577-40-6,37180-49-7,37180-53-3,57538-70-2,96779-61-2,98392-36-0,107657-07-8,107657-09-0,130195-96-9,141611-58-7,144607-24-9,144607-27-2,150654-15-2,150654-16-3) + Acetic acid (2R,4aR,6S,7R,8S,8aS)-2-(4-bromo-phenyl)-8-hydroxy-6-methoxy-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester + Benzoic acid (2R,4aR,6S,7R,8S,8aS)-2-(4-bromo-phenyl)-8-hydroxy-6-methoxy-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

Guidance literature:

methyl 2,3,4,6-tetrakis-O-trimethylsilyl-α-D-glucopyranoside; 4-chlorobenzaldehyde; benzaldehyde; 4-bromo-benzaldehyde; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 2h; Molecular sieve; Combinatorial reaction / High throughput screening (HTS);

With triethylsilane; β-naphthaldehyde; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 5h;

acetic anhydride; benzoic acid anhydride; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; trimethylsilyl trifluoromethanesulfonate; more than 3 stages; Product distribution / selectivity;

upstream raw materials:

methyl 2,3,4,6-tetrakis-O-trimethylsilyl-α-D-glucopyranoside

acetic anhydride

4-chlorobenzaldehyde

benzaldehyde