2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

Base Information

Chemical Name:2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone
CAS No.:107686-27-1
Molecular Formula:C₁₅H₁₄Br₂O₄
Molecular Weight:418.082
Hs Code.:

Synonyms:2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

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Chemical Property of 2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

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Technology Process of 2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

There total 1 articles about 2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5307-05-1
1-hydroxy-4-methoxy-2-methylbenzene

: 107686-27-1
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Br₂, AcOH / Ambient temperature

2: 1.) NaOMe / 1.) DMSO, RT, 10 min, 2.) DMSO, 6 h

With bromine; sodium methylate; acetic acid;

Reference yield: 88.0%

: 107-21-1
ethylene glycol

: 107686-27-1
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

: 81805-50-7
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 72h; Heating;

Reference yield:

: 107686-27-1
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

: 5090-88-0
mansonone F

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / p-TsOH / benzene / 72 h / Heating

2: 61 percent / BuLi / tetrahydrofuran; hexane; diethyl ether / 2.5 h / -78 - 20 °C

3: 98 percent / Fe₂(CO)9 / benzene / 4 h / Heating

4: 100 percent / 2 M aq. HClO₄ / CH₂Cl₂ / 5 h / Ambient temperature

5: 75 percent / diethyl ether / 0.25 h / Ambient temperature

6: 15 percent / AgO, 6 M aq. HNO₃ / dioxane / 0.25 h / Ambient temperature

7: 56 percent / H₂SO₄ / ethanol / 0.5 h / Heating

With silver(II) oxide; n-butyllithium; perchloric acid; diiron nonacarbonyl; sulfuric acid; nitric acid; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; hexane; dichloromethane; benzene;