2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

Base Information

Chemical Name:2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal
CAS No.:81805-50-7
Molecular Formula:C₁₇H₁₈Br₂O₅
Molecular Weight:462.135
Hs Code.:

Synonyms:2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

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Technology Process of 2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

There total 4 articles about 2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 107-21-1
ethylene glycol

: 107686-27-1
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone

: 81805-50-7
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 72h; Heating;

Reference yield:

: 81805-55-2
chloromethyl 5-methyl-2-furyl ketone

: 81805-50-7
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOMe / 1.) DMSO, RT, 10 min, 2.) DMSO, 6 h

2: 88 percent / p-TsOH / benzene / 72 h / Heating

With sodium methylate; toluene-4-sulfonic acid; In benzene;

Reference yield:

: 5307-05-1
1-hydroxy-4-methoxy-2-methylbenzene

: 81805-50-7
2-(2,3-dibromo-4-methoxy-6-methylphenoxy)-1-(5-methylfuran-2-yl)ethanone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Br₂, AcOH / Ambient temperature

2: 1.) NaOMe / 1.) DMSO, RT, 10 min, 2.) DMSO, 6 h

3: 88 percent / p-TsOH / benzene / 72 h / Heating

With bromine; sodium methylate; toluene-4-sulfonic acid; acetic acid; In benzene;